The department's instructional laboratories for chemical
engineering majors contain modern analytical instruments and
process engineering apparatus. Most equipment, such as the
computer-coupled, closed-loop, continuous-flow distillation unit,
features advanced microprocessor design, representing the
state-of-the-art in automation.
As a special feature, the department's
research equipment is available for students conducting undergraduate research, whether by individual arrangement or through programs such as the Chemical and Biochemical Engineering Research Scholars Academy and the James J. Slade Scholars Program. The impetus for this unique offering stems from the
department's strong commitment to research and its active
involvement with sponsored research projects at the university and
state high-tech centers. Research is in such areas as advanced materials, bioengineering and biotechnology,
sustainable energy and biofuels, process systems engineering, kinetics and catalysis, pharmaceutical engineering, and polymer science.
The department's major instructional laboratories
include a chemical process engineering laboratory, a biochemical
engineering laboratory, and pharmaceutical engineering laboratories.
The Chemical-Process Engineering Laboratory is
devoted to the study of chemical reactions and physical phase
separations for multicomponent systems. Typical apparatus includes
distillation, gas absorption, liquid extraction, wiped-film
evaporation, falling-film evaporation, and computer-coupled process
control units. Special devices are used for the study of fluid flow in
pipe systems and heat transfer in heat exchangers. Analyses of changes
in chemical compositions are aided by gas chromatographs, UV and IR
spectrophotometers, refractometers, and many other modern analytical
instruments.
The department's Biochemical Engineering Laboratory is devoted to the study of biochemical engineering processes
and the detection and separation of biospecies resulting from these
bioprocesses. Specific experiments in enzyme and fermentation kinetics,
for batch and continuous systems, are provided. This fully equipped biolaboratory contains a wide range of analytical instruments and
specialized devices, including a Pharmacia Fine-Chemicals
microprocessor-controlled and automated liquid chromatograph analyzer,
and a computer-coupled BIOFLOW III fermentor system.
The Reaction Engineering Laboratory contains custom built quartz tube reactors with attached Raman, UV, and IR spectrophotometers for in situ measurements. Gas and liquid chromatography are also available. For synthetic work, there is a wide range of synthetic equipment to prepare various nanostructured materials, catalysts, and electrocatalysts. It includes rotovaps, vacuum lines, centrifuges, ultrasonicators, ovens, tube furnaces, and oven furnaces.
The Soft Materials Characterization Laboratory
contains various equipment, especially for particle synthesis and characterization, including an optical microscope, UV/Vis spectrophotometer, benchtop Nutsche filter, and Abbe refractometer, as well as syringe pumps, filters, blenders, and homogenizers. There is additional catalyst manufacturing equipment, such as impregnators, and drying equipment. There also is a facility for the investigation of
theoretical properties of polymers and soft materials by thermodynamics and statistical
mechanics and other methods, and for computer modeling of their
behavior.
The Pharmaceutical Engineering Laboratories are environmentally controlled and capable of reproducing moisture and temperature conditions used in pharmaceutical manufacturing. In total, these modern facilities contain over 20 laminar flow hoods, three temperature and humidity-controlled rooms, and laboratory bench space designed for both small and large equipment and instruments. Equipment that relates to the synthetic production and purification of active pharmaceutical ingredients include stirred tanks, crystallizers, granulators, a rotating fluidized bed coater, dryers, a wipe-film evaporator, batch distillation column, liquid-liquid extractors, and a Particle Imaging Velocimeter/Laser-Induced Fluorometer. The research facility currently contains extensive solids-processing equipment used by major pharmaceutical, food, and agrochemical companies for the formulation of new products. This combination of equipment is rare in educational engineering programs. For example, the program currently owns a pan-coater, two tablet press, mills, fluidized-bed equipment, and essentially every category of powder blenders used in the industry, including a five-cubic-foot capacity ribbon blender and a 10-cubic-foot capacity bin blender. The Continuous Pharmaceutical Advanced Manufacturing Laboratory is a fully integrated, control-enabled, commercial-scale pilot plant for continuous manufacturing. This facility is the only one of its kind at a university anywhere in the world and has served as a model for numerous commercial facilities around the world.